A NOVEL STUDY ON THE SYNTHESIS, CHARACTERIZATION, AND PHOTOCATALYTIC ACTIVITY OF CeO2 NANOPARTICLES

Nazlı Türkten; Yunus Karataş

doi:10.17780/ksujes.1369994

TR EN

CeO2 NANOTANECİKLERİNİN SENTEZİ, KARAKTERİZASYONU VE FOTOKATALİTİK AKTİVİTESİ

Öz

Boya içeren endüstriyel atık suyunun yeterli bir arıtma işlemi yapılmadan boşaltılması sonucunda önemli çevre ve su kirliliği oluşabilir. Yarı iletken fotokataliz, atık sulardaki organik boyaların parçalanması amacıyla yaygın olarak kullanılan uygun bir teknolojidir. Bu çalışmada, CeO2 nanotanecikleri basit bir çöktürme yöntemi kullanılarak hazırlanmıştır. Fourier dönüşümlü kızılötesi spektroskopisi-zayıflatılmış toplam yansıma (FTIR-ATR), Raman spektroskopisi, X-ışını difraktometresi (XRD) ve taramalı elektron mikroskobu (SEM) yöntemleri kullanılarak CeO2 nanotaneciklerinin yapısal ve morfolojik özellikleri belirlenmiştir. FTIR spektrumunda yer alan karakteristik bandların varlığı CeO2 oluşumunun başarılı bir şekilde gerçekleştiğini göstermiştir. Scherrer eşitliği kullanılarak kristal tanecik boyutu 10 nm olarak hesaplanmıştır. SEM görüntüleri, CeO2’nin morfolojisinin yüzeyde çok az bir topaklanma olsa da neredeyse küresel taneciklerden oluştuğunu ortaya çıkarmıştır. Brunauer-Emmett-Teller (BET) yöntemi kullanılak CeO2 nanotaneciklerinin spesifik yüzey alanı (11 m2/g) belirlenmiştir. CeO2 nanotaneciklerinin etkinliği, UV ışığı altında Rhodamin B (Rh B) boyasına karşı fotokatalitik aktiviteleri incelenerek saptanmıştır. Elde edilen sonuçlar, CeO2 nanotaneciklerinin endüstriyel atıksu arıtımında kullanılabilecek, ileriye dönük ümit vaat eden bir katalizör olduğunu göstermiştir.

Anahtar Kelimeler

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Details

Primary Language

English

Subjects

Environmental Engineering (Other)

Journal Section

Research Article

Authors

Nazlı Türkten ^*
0000-0001-9343-3697
Türkiye

Yunus Karataş
0000-0002-3826-463X
Türkiye

Publication Date

March 3, 2024

Submission Date

October 2, 2023

Acceptance Date

December 28, 2023

Published in Issue

Year 1970 Volume: 27 Number: 1

DOI

https://doi.org/10.17780/ksujes.1369994

IZ

https://izlik.org/JA34YG56RT

Cite

RIS / Bibtex

APA

Türkten, N., & Karataş, Y. (2024). A NOVEL STUDY ON THE SYNTHESIS, CHARACTERIZATION, AND PHOTOCATALYTIC ACTIVITY OF CeO2 NANOPARTICLES. Kahramanmaraş Sütçü İmam Üniversitesi Mühendislik Bilimleri Dergisi, 27(1), 190-198. https://doi.org/10.17780/ksujes.1369994

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A NOVEL STUDY ON THE SYNTHESIS, CHARACTERIZATION, AND PHOTOCATALYTIC ACTIVITY OF CeO2 NANOPARTICLES

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Öz

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